Wednesday, March 11, 2020

NMR essays

NMR essays Instrument: JEOL 270 MHZ Nuclear Magnetic Resonance Spectrometer Nuclear magnetic resonance is a phenomenon, which occurs when the nuclei of certain atoms are immersed in a static magnetic field and exposed to a second oscillating magnetic field. Some nuclei experience this phenomenon, and others do not, dependent upon whether they possess a property called spin. Most of the matter you can examine with NMR is composed of molecules. Molecules are composed of atoms .Not all nuclei possess the property called spin Spectroscopy is the study of the interaction of electromagnetic radiation with matter. Nuclear magnetic resonance spectroscopy is the use of the NMR phenomenon to study physical, chemical, and biological properties of matter. As a consequence, NMR spectroscopy finds applications in several areas of science. NMR spectroscopy is used to study chemical structure using simple one-dimensional techniques. Two-dimensional techniques are used to determine the structure of more complicated molecules. Units of time are seconds (s). Angles are reported in degrees (o) and in radians (rad). There are 2 radians in 360o. The absolute temperature scale in Kelvin (K) is used in NMR. The Kelvin temperature scale is equal to the Celsius scale reading plus 273.15. 0 K is characterized by the absence of molecular motion. There are no degrees in the Kelvin temperature unit. Magnetic field strength (B) is measured in Tesla (T). The unit of energy (E) is the Joule (J Spin is a fundamental property of nature like electrical charge or mass. Spin comes in multiples of 1/2 and can be + or -. Protons, electrons, and neutrons possess spin. Individual unpaired electrons, protons, and neutrons each possess a spin of 1/2. In the deuterium atom ( 2H ), with one unpaired electron, one unpaired proton, and one unpaired neutron, the total electronic spin = 1/2 and the total nuclear ...

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